Inficon 3000 Micro GC Gas Analyzer Reference Guide Bedienungsanleitung

REFERENCE GUIDE3000 Micro GCGas AnalyzerPN 074-558-P1ACover Page

TOC - 2 PN 074-558-P1A3000 Micro GC Guides3000 Micro GC Guide 10Setting Annotations...

22 - 2 PN 074-558-P1A 3000 Micro GC Guides4Before installing the digital I/O module, prepare the instrument for service. Lower the heated inlets, inj

22 - 3PN 074-558-P1A3000 Micro GC Guides 8 Remove the two screws on each side of the top cover using a Torx T-20 or Phillips Head screwdriver

22 - 4 PN 074-558-P1A 3000 Micro GC Guides11 Disconnect the ribbon cable from the communication board.12 Remove the two screws fastening the module t

22 - 5PN 074-558-P1A3000 Micro GC Guides 15 Attach one end of the ribbon cable to digital I/O module position J2.16 Attach the other end of t

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23 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 23Replacing the Battery Cable Fuse on a PortableInstrumentTable 23-1 Replacing

23 - 2 PN 074-558-P1A 3000 Micro GC Guides6 Locate the battery cable fuse.7 Locate the battery cable fuse positions.8 Disconnect the battery cable fu

23 - 3PN 074-558-P1A3000 Micro GC Guides 11 Next, connect both Plug B connectors to Position 3.12 Connect the Plug C connector to Position 2.

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1 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 1Configuring a PC for a Direct Connection to3000 Micro GC via the Crossover Cable

1 - 2 PN 074-558-P1A 3000 Micro GC Guides5 In the Local Area Connection Status window, click Properties.6 In the Local Area Connection Properties win

1 - 3PN 074-558-P1A3000 Micro GC Guides 7 In the Internet Protocol (TCP/IP) Properties window, select Use the following IP address.8 Type the

1 - 4 PN 074-558-P1A 3000 Micro GC Guides12 Click (Windows) Start >> Run.13 In the Run window, in the Open: box, type ping 10.1.1.101. Click OK

2 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 2Connecting to 3000 Micro GCvia the Static IP AddressTable 2-1 Connecting to the

2 - 2 PN 074-558-P1A 3000 Micro GC Guides6 In the Local Area Connection Status window, click Properties.7 The Local Area Connection Properties window

2 - 3PN 074-558-P1A3000 Micro GC Guides 8 In the Internet Protocol (TCP/IP) Properties window, select Use the following IP address.9 Type the

2 - 4 PN 074-558-P1A 3000 Micro GC Guides13 Click (Windows) Start >> Run.14 In the Run window, in the Open: box, type ping 192.168.1.99. Click

3 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 3Changing the Instrument IP AddressTable 3-1 Changing the Instrument IP AddressS

3 - 2 PN 074-558-P1A 3000 Micro GC Guides6 Type the desired changes to the IP address and click Submit. NOTE: Consult an IT professional to assist wi

3 - 3PN 074-558-P1A3000 Micro GC Guides 10 Verify from the Command Prompt window that the PC is receiving data packetsfrom the instrument. NO

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4 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 4Changing the Carrier Gas ConfigurationTable 4-1 Changing the carrier gas config

4 - 2 PN 074-558-P1A 3000 Micro GC Guides6 Under Connection, select the carrier gas connection that corresponds to the desired GC module. Click Submi

4 - 3PN 074-558-P1A3000 Micro GC Guides 9 When the column temperatures are below 60ºC, click Continue.NOTE: Closing the browser or clicking b

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5 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 5Installing EZ IQTable 5-1 Installing EZ IQStep Description1 Insert the EZ IQ In

5 - 2 PN 074-558-P1A 3000 Micro GC Guides5 The EZ IQ Setup - Select Program Folder window will display. In the Program Folder: box, type in a name fo

5 - 3PN 074-558-P1A3000 Micro GC Guides 8 When the installation is complete, the EZ IQ Setup Reboot to Complete Setup window will display. Cl

www.inficon.com [email protected] ©2013 INFICONREFERENCE GUIDE3000 Micro GCGas AnalyzerPN 074-558-P1ATitle Page

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6 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 6Configuring a 3000 Micro GC with EZ IQTable 6-1 Configuring 3000 Micro GC with

6 - 2 PN 074-558-P1A 3000 Micro GC Guides5 Double-click the INFICON 3000 Micro GC icon in the Configured modules panel to open the INFICON 3000 Micro

7 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 73000 Micro GC Method SetupTable 7-1 Creating a methodStep Description1 It is po

7 - 2 PN 074-558-P1A 3000 Micro GC Guides3 The Instrument Setup window will display. It will display parameters that can be edited.NOTE: The Instrume

7 - 3PN 074-558-P1A3000 Micro GC Guides 4 Click the Trigger tab. In the Type: list, select the trigger type. If the sample run will be initi

7 - 4 PN 074-558-P1A 3000 Micro GC Guides7 Click Control >> Instrument Status to view the status of the instrument.NOTE: The status will read N

8 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 8Running a SampleTable 8-1 Running a sampleStep Description1 To start the run, c

8 - 2 PN 074-558-P1A 3000 Micro GC Guides4 Select a path for storage of data files by selecting the folder icon located on the right of the Data path

9 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 9Integrating ChromatogramsTable 9-1 Integrating ChromatogramsStep Description1 I

TrademarksThe trademarks of the products mentioned in this manual are held by the companies that produce them.3000 Micro GC® and Opening The Field To

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10 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 10Setting AnnotationsTable 10-1 Setting AnnotationsStep Description1 In EZ IQ,

10 - 2 PN 074-558-P1A 3000 Micro GC Guides7 Select the check boxes to display Baseline, USP Width, Retention Time Window, Show Undetected Named Peaks

11 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 11Qualifying Peaks and GroupsTable 11-1 Qualify peaks and groupsStep Descriptio

11 - 2 PN 074-558-P1A 3000 Micro GC Guides3 The Peak/Group Tables window will display. There are tabs for Named Peaks and Groups. On the Named Peaks

12 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 12Adjusting Retention Time WindowsTable 12-1 Adjusting retention time windowsSt

12 - 2 PN 074-558-P1A 3000 Micro GC Guides2 A blue Adjust Retention Time Window window will display. Click directly on the desired retention time win

13 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 13Conducting a Single Level CalibrationTable 13-1 Conduct a single level calibr

13 - 2 PN 074-558-P1A 3000 Micro GC Guides7 To calibrate, click Analysis >> Analysis/Single Level Calibration.8 The Analysis/Single Level Calib

13 - 3PN 074-558-P1A3000 Micro GC Guides 15 When finished, click Start.16When the analysis is complete, the chromatogram will be integrated,

PN 074-558-P1A3000 Micro GC GuidesPurpose of this Reference Guide3000 Micro GC Guides are not intended to replace the 3000 Micro GC Operating Manual

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14 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 14Conducting a Multiple Level CalibrationTable 14-1 Conduct a multiple level ca

14 - 2 PN 074-558-P1A 3000 Micro GC Guides6 To calibrate, click Analysis >> Analysis/Single Level Calibration.7 The Analysis/Single Level Calib

14 - 3PN 074-558-P1A3000 Micro GC Guides 15 When the analysis is complete, the chromatogram will be integrated. The areas for the peaks ident

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15 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 15Calibration with Average ReplicatesTable 15-1 Conducting a calibration with r

15 - 2 PN 074-558-P1A 3000 Micro GC Guides6 To calibrate, click Analysis >> Analysis/Single Level Calibration.7 The Analysis/Single Level Calib

15 - 3PN 074-558-P1A3000 Micro GC Guides 14 When finished, click Start.15 When the analysis is complete, the chromatogram will be integrated,

15 - 4 PN 074-558-P1A 3000 Micro GC Guides18 On the calibration curve, a blue point represents a single replicate, and a green point represents the a

16 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 16Customizing a Method ReportTable 16-1 Customize a reportStep Description1 The

PN 074-558-P1A 3000 Micro GC GuidesDefinition ofNote, Hint, Danger, Warning and Caution ParagraphsNOTE: These messages contain pertinent information t

16 - 2 PN 074-558-P1A 3000 Micro GC Guides5 The Open Report Template File window will prompt to open a template file, such as External Standard.srp,

16 - 3PN 074-558-P1A3000 Micro GC Guides 8 The Save Method Custom Report As window will display. In the File Name: box, type a method report

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17 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 17Customizing an ESTD ReportTable 17-1 Customizing an external standard (ESTD)

17 - 2 PN 074-558-P1A 3000 Micro GC Guides5 To edit the report, right-click and select options such as Insert Field, Insert Graph, Insert Report, and

17 - 3PN 074-558-P1A3000 Micro GC Guides 8 To view the ESTD report, click Reports >> View >> External Standard.9 To print the EST

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18 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 18Changing a Standard ModuleTable 18-1 Changing a standard moduleStep Descripti

18 - 2 PN 074-558-P1A 3000 Micro GC Guides3 Click Remove.NOTE: Once a Standard GC module is decommissioned, it can not be used again until it is reco

18 - 3PN 074-558-P1A3000 Micro GC Guides 6 Do not turn off power. Allow three minutes for the instrument to shut down. A The system is shutti

PN 074-558-P1A3000 Micro GC GuidesHow To Contact Customer SupportWorldwide support information regarding: Technical Support, to contact an applicati

18 - 4 PN 074-558-P1A 3000 Micro GC Guides9 Loosen the thumbscrews in the manifold cover plate.10 Remove the manifold cover plate. In the two screw d

18 - 5PN 074-558-P1A3000 Micro GC Guides 12 Use a T-20 screwdriver (PN 5182-3468) to loosen the screw in the inlet manifold fitting at the ba

18 - 6 PN 074-558-P1A 3000 Micro GC Guides15 Tilt the back of the GC module up until the mounting flange clears the alignment pins. Slide the GC modu

18 - 7PN 074-558-P1A3000 Micro GC Guides 18 Inspect the GC module mounting flange fitting to verify all new O-rings on the replacement GC mod

18 - 8 PN 074-558-P1A 3000 Micro GC Guides20 Lower the back of the GC module into position until there is enough clearance to position it into place

18 - 9PN 074-558-P1A3000 Micro GC Guides 21 Re-connect the communications cables, as shown below. NOTE: Do not connect more than two GC modul

18 - 10 PN 074-558-P1A 3000 Micro GC Guides27 In the web browser address bar, type the instrument IP address.28 Click the Utilities tab.29 Click Chan

18 - 11PN 074-558-P1A3000 Micro GC Guides 32 After selecting the address, click Restart.33 A The system is shutting down... message is displa

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19 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 19Changing a Performance Enhanced ModuleTable 19-1 Changing a Performance Enhan

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19 - 2 PN 074-558-P1A 3000 Micro GC Guides4 Carefully remove the manifold insulation. Save for reuse.NOTE: In the Portable 3000 Micro GC, the DC-DC c

19 - 3PN 074-558-P1A3000 Micro GC Guides 7 Disconnect the communication cables leading from the GC modules, if present, to the communications

19 - 4 PN 074-558-P1A 3000 Micro GC Guides10 On the replacement module, set the Performance Enhanced GC module address by setting the DIP switch on t

19 - 5PN 074-558-P1A3000 Micro GC Guides 12 Inspect the GC module mounting flange fitting to verify all new O-rings on the replacement GC mod

19 - 6 PN 074-558-P1A 3000 Micro GC Guides14 Lower the back of the GC module into position until there is enough clearance to position it into place

19 - 7PN 074-558-P1A3000 Micro GC Guides 15 Re-connect the communications cables. NOTE: Do not connect more than two GC modules in series per

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20 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 20Replacing a Standard Module with aPerformance Enhanced ModuleTable 20-1 Chang

20 - 2 PN 074-558-P1A 3000 Micro GC Guides4 Click Remove.NOTE: Once a Standard GC module is decommissioned, it cannot be used until it is recommissio

20 - 3PN 074-558-P1A3000 Micro GC Guides 8 Remove the two screws on each side of the top cover using a Torx T-20 or Phillips Head screwdriver

TOC - 1PN 074-558-P1A3000 Micro GC Guides Table Of ContentsCover PageTitle PageTrademarksDisclaimerCopyrightPurpose of this Reference GuideDefinitio

20 - 4 PN 074-558-P1A 3000 Micro GC Guides12 Use a T-20 screwdriver to loosen the screw in the inlet manifold fitting at the back of the GC module.13

20 - 5PN 074-558-P1A3000 Micro GC Guides 15 Tilt the back of the GC module up until the mounting flange clears the alignment pins. Slide the

20 - 6 PN 074-558-P1A 3000 Micro GC Guides17 On the new module, set the Performance Enhanced GC module address by setting the DIP switch on the upper

20 - 7PN 074-558-P1A3000 Micro GC Guides 19 Inspect the GC module mounting flange fitting to verify all new O-rings on the replacement GC mod

20 - 8 PN 074-558-P1A 3000 Micro GC Guides21 Lower the back of the GC module into position until there is enough clearance to position it into place

20 - 9PN 074-558-P1A3000 Micro GC Guides 22 Re-connect the communications cables. NOTE: Do not connect more than two GC modules in series per

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21 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 21Testing Instrument Flow RatesTable 21-1 Test instrument flow ratesStep Descri

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22 - 1PN 074-558-P1A3000 Micro GC Guides 3000 Micro GC Guide 22Installing the Digital I/O ModuleTable 22-1 Installing the digital I/O module